Erratum: Total synthesis of natural hyacinthacine C5 and six related hyacinthacine C5 epimers (The Journal of Organic Chemistry (2018) 83:10 (5558-5576) DOI: 10.1021/acs.joc.8b00585)

Anthony W. Carroll; Kongdech Savaspun; Anthony C. Willis; Masako Hoshino; Atsushi Kato; Stephen G. Pyne

doi:10.1021/acs.joc.0c00855

Erratum: Total synthesis of natural hyacinthacine C5 and six related hyacinthacine C5 epimers (The Journal of Organic Chemistry (2018) 83:10 (5558-5576) DOI: 10.1021/acs.joc.8b00585)

Anthony W. Carroll, Kongdech Savaspun, Anthony C. Willis, Masako Hoshino, Atsushi Kato, Stephen G. Pyne^*

^*この論文の責任著者

薬剤部

研究成果: ジャーナルへの寄稿 › コメント/討論

抄録

In the section: General Method for the Formation of a Cyclic Sulfate, the reagent SOCl₂ should be replaced by SO₂Cl₂. This reagent (SO₂Cl₂) is correctly shown in the original schemes. The correct text is General Method for the Formation of a Cyclic Sulfate. (3aR,4R,6R,7R,8R,8aS,8bS)-7,8-Bis(benzyloxy)-6-((benzyloxy)methyl)-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (48). To a solution of the diol 46 (48 mg, 0.098 mmol) in anhydrous CH₂Cl₂2 (5 mL) under a nitrogen atmosphere was added at 0 °C, Et3N (35 μL, 0.25 mmol), and then SO₂Cl₂ (12 &mulL, 0.15 mmol) dropwise.

本文言語	英語
ページ（範囲）	6242
ページ数	1
ジャーナル	Journal of Organic Chemistry
巻	85
号	9
DOI	https://doi.org/10.1021/acs.joc.0c00855
出版ステータス	出版済み - 2020/05/01

ASJC Scopus 主題領域

有機化学

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10.1021/acs.joc.0c00855

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「Erratum: Total synthesis of natural hyacinthacine C5 and six related hyacinthacine C5 epimers (The Journal of Organic Chemistry (2018) 83:10 (5558-5576) DOI: 10.1021/acs.joc.8b00585)」の研究トピックを掘り下げます。これらがまとまってユニークなフィンガープリントを構成します。

引用スタイル

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abstract = "In the section: General Method for the Formation of a Cyclic Sulfate, the reagent SOCl2 should be replaced by SO2Cl2. This reagent (SO2Cl2) is correctly shown in the original schemes. The correct text is General Method for the Formation of a Cyclic Sulfate. (3aR,4R,6R,7R,8R,8aS,8bS)-7,8-Bis(benzyloxy)-6-((benzyloxy)methyl)-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (48). To a solution of the diol 46 (48 mg, 0.098 mmol) in anhydrous CH2Cl22 (5 mL) under a nitrogen atmosphere was added at 0 °C, Et3N (35 μL, 0.25 mmol), and then SO2Cl2 (12 &mulL, 0.15 mmol) dropwise.",

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Erratum: Total synthesis of natural hyacinthacine C5 and six related hyacinthacine C5 epimers (The Journal of Organic Chemistry (2018) 83:10 (5558-5576) DOI: 10.1021/acs.joc.8b00585). / Carroll, Anthony W.; Savaspun, Kongdech; Willis, Anthony C. その他.
In: Journal of Organic Chemistry, Vol. 85, No. 9, 01.05.2020, p. 6242.

研究成果: ジャーナルへの寄稿 › コメント/討論

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