TY - JOUR
T1 - Erratum
T2 - Total synthesis of natural hyacinthacine C5 and six related hyacinthacine C5 epimers (The Journal of Organic Chemistry (2018) 83:10 (5558-5576) DOI: 10.1021/acs.joc.8b00585)
AU - Carroll, Anthony W.
AU - Savaspun, Kongdech
AU - Willis, Anthony C.
AU - Hoshino, Masako
AU - Kato, Atsushi
AU - Pyne, Stephen G.
N1 - Publisher Copyright:
© 2020 American Chemical Society. All rights reserved.
PY - 2020/5/1
Y1 - 2020/5/1
N2 - In the section: General Method for the Formation of a Cyclic Sulfate, the reagent SOCl2 should be replaced by SO2Cl2. This reagent (SO2Cl2) is correctly shown in the original schemes. The correct text is General Method for the Formation of a Cyclic Sulfate. (3aR,4R,6R,7R,8R,8aS,8bS)-7,8-Bis(benzyloxy)-6-((benzyloxy)methyl)-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (48). To a solution of the diol 46 (48 mg, 0.098 mmol) in anhydrous CH2Cl22 (5 mL) under a nitrogen atmosphere was added at 0 °C, Et3N (35 μL, 0.25 mmol), and then SO2Cl2 (12 &mulL, 0.15 mmol) dropwise.
AB - In the section: General Method for the Formation of a Cyclic Sulfate, the reagent SOCl2 should be replaced by SO2Cl2. This reagent (SO2Cl2) is correctly shown in the original schemes. The correct text is General Method for the Formation of a Cyclic Sulfate. (3aR,4R,6R,7R,8R,8aS,8bS)-7,8-Bis(benzyloxy)-6-((benzyloxy)methyl)-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (48). To a solution of the diol 46 (48 mg, 0.098 mmol) in anhydrous CH2Cl22 (5 mL) under a nitrogen atmosphere was added at 0 °C, Et3N (35 μL, 0.25 mmol), and then SO2Cl2 (12 &mulL, 0.15 mmol) dropwise.
UR - http://www.scopus.com/inward/record.url?scp=85084834700&partnerID=8YFLogxK
U2 - 10.1021/acs.joc.0c00855
DO - 10.1021/acs.joc.0c00855
M3 - コメント/討論
AN - SCOPUS:85084834700
SN - 0022-3263
VL - 85
SP - 6242
JO - Journal of Organic Chemistry
JF - Journal of Organic Chemistry
IS - 9
ER -