TY - JOUR
T1 - Erratum
T2 - Corrected Structure of Natural Hyacinthacine C1 via Total Synthesis (Journal of Natural Products (2019) 82: 2 (358−367) DOI: 10.1021/acs.jnatprod.8b00879)
AU - Carroll, Anthony W.
AU - Willis, Anthony C.
AU - Hoshino, Masako
AU - Kato, Atsushi
AU - Pyne, Stephen G.
N1 - Publisher Copyright:
© 2020 American Chemical Society and American Society of Pharmacognosy.
PY - 2020/5/22
Y1 - 2020/5/22
N2 - Metrics & More. Article Recommendations. Page 365, For the synthesis of (3aR,4R,6R,7R,8S,8aS,8bS)-7,8-Bisbenzyloxy-6-[(benzyloxy)-methyl]-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (26), the reagent SOCl2 should be replaced by SO2Cl2. This reagent (SO2Cl2) is correctly shown in the Scheme. The correct text is: (3aR,4R,6R,7R,8S,8aS,8bS)-7,8-Bisbenzyloxy-6-[(benzyloxy)-methyl]-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (26). To a solution of the diol 25 (25 mg, 0.0511 mmol) in anhydrous CH2Cl2 (5 mL) under a nitrogen atmosphere was added at 0 °C Et3 N (18 μL, 0.128 mmol), then SO2Cl2 (1.0 M solution in CH2Cl2, 0.0766 μL, 0.0766 mmol) dropwise.
AB - Metrics & More. Article Recommendations. Page 365, For the synthesis of (3aR,4R,6R,7R,8S,8aS,8bS)-7,8-Bisbenzyloxy-6-[(benzyloxy)-methyl]-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (26), the reagent SOCl2 should be replaced by SO2Cl2. This reagent (SO2Cl2) is correctly shown in the Scheme. The correct text is: (3aR,4R,6R,7R,8S,8aS,8bS)-7,8-Bisbenzyloxy-6-[(benzyloxy)-methyl]-4-methylhexahydro-4H-[1,3,2]dioxathiolo[4,5-a]-pyrrolizine 2,2-dioxide (26). To a solution of the diol 25 (25 mg, 0.0511 mmol) in anhydrous CH2Cl2 (5 mL) under a nitrogen atmosphere was added at 0 °C Et3 N (18 μL, 0.128 mmol), then SO2Cl2 (1.0 M solution in CH2Cl2, 0.0766 μL, 0.0766 mmol) dropwise.
UR - http://www.scopus.com/inward/record.url?scp=85084312835&partnerID=8YFLogxK
U2 - 10.1021/acs.jnatprod.0c00389
DO - 10.1021/acs.jnatprod.0c00389
M3 - コメント/討論
C2 - 32315182
AN - SCOPUS:85084312835
SN - 0163-3864
VL - 83
SP - 1733
JO - Journal of Natural Products
JF - Journal of Natural Products
IS - 5
ER -