The reaction of diazines with allyltributyltin via N-alkoxycarbonyldiazinium salts

Takashi Itoh; Hiroshi Hasegawa; Kazuhiro Nagata; Yûji Matsuya; Akio Ohsawa

doi:10.3987/com-93-s92

The reaction of diazines with allyltributyltin via N-alkoxycarbonyldiazinium salts

Takashi Itoh^*, Hiroshi Hasegawa, Kazuhiro Nagata, Yûji Matsuya, Akio Ohsawa

^*この論文の責任著者

薬品製造学研究室

研究成果: ジャーナルへの寄稿 › 学術論文 › 査読

14 被引用数 (Scopus)

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Pyridazines were allowed to react with allyltributyltin in the presence of chloroformate to give 1-alkoxycarbonyl-6-allyl- and 1-alkoxycarbonyl-4-allyldihydro-pyridazines as major and minor products, respectively. The reaction was applied to other diazines, and tetrahydro-adducts were obtained in the case of pyrimidine and pyrazine. Benzo-fused diazines also reacted in the same manner to afford the allyl-adducts in good yields.

本文言語	英語
ページ（範囲）	709-713
ページ数	5
ジャーナル	Heterocycles
巻	37
号	2
DOI	https://doi.org/10.3987/com-93-s92
出版ステータス	出版済み - 1994/03/03

ASJC Scopus 主題領域

分析化学
薬理学
有機化学

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10.3987/com-93-s92

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abstract = "Pyridazines were allowed to react with allyltributyltin in the presence of chloroformate to give 1-alkoxycarbonyl-6-allyl- and 1-alkoxycarbonyl-4-allyldihydro-pyridazines as major and minor products, respectively. The reaction was applied to other diazines, and tetrahydro-adducts were obtained in the case of pyrimidine and pyrazine. Benzo-fused diazines also reacted in the same manner to afford the allyl-adducts in good yields.",

author = "Takashi Itoh and Hiroshi Hasegawa and Kazuhiro Nagata and Y{\^u}ji Matsuya and Akio Ohsawa",

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AU - Itoh, Takashi

AU - Hasegawa, Hiroshi

AU - Nagata, Kazuhiro

AU - Matsuya, Yûji

AU - Ohsawa, Akio

PY - 1994/3/3

Y1 - 1994/3/3

N2 - Pyridazines were allowed to react with allyltributyltin in the presence of chloroformate to give 1-alkoxycarbonyl-6-allyl- and 1-alkoxycarbonyl-4-allyldihydro-pyridazines as major and minor products, respectively. The reaction was applied to other diazines, and tetrahydro-adducts were obtained in the case of pyrimidine and pyrazine. Benzo-fused diazines also reacted in the same manner to afford the allyl-adducts in good yields.

AB - Pyridazines were allowed to react with allyltributyltin in the presence of chloroformate to give 1-alkoxycarbonyl-6-allyl- and 1-alkoxycarbonyl-4-allyldihydro-pyridazines as major and minor products, respectively. The reaction was applied to other diazines, and tetrahydro-adducts were obtained in the case of pyrimidine and pyrazine. Benzo-fused diazines also reacted in the same manner to afford the allyl-adducts in good yields.

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The reaction of diazines with allyltributyltin via N-alkoxycarbonyldiazinium salts

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