Facile synthesis of zeolites under an atmospheric reflux system

Xu Sun, Jiayuan Wang, Yujia Jiang, Elton Maturura, Wenhang Wang, Ruiqin Yang, Chuang Xing*, Jiangang Chen*, Noritatsu Tsubaki*

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

4 Scopus citations

Abstract

Traditionally zeolites are produced under long aging processes and high autogenous pressure reactions associated with a lot of safety concerns and explosion risks. Herein, a facile zeolite synthesis method under atmospheric pressure using a reflux system is reported. The zeolite gel crystallizes rapidly under the synthesis conditions of heating, stirring, and reflux in an oil bath. We have successfully synthesized LTA, FAU, MFI, and BEA zeolites. This technique not only eliminates the potential risks associated with pressure vessels but also greatly improves the synthesis rate and speeds up the production cycle. This synthesis strategy provides a new, safe and rapid way of synthesizing zeolites.

Original languageEnglish
Article number111646
JournalMicroporous and Mesoporous Materials
Volume331
DOIs
StatePublished - 2022/01

Keywords

  • Atmospheric synthesis
  • Facile synthesis
  • Reflux system
  • Zeolite

ASJC Scopus subject areas

  • General Chemistry
  • General Materials Science
  • Condensed Matter Physics
  • Mechanics of Materials

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