Fabrication of ZrN-hBN composite ceramics by pulse current pressure sintering and their tribological behavior

Masateru Nose*, Hirofumi Suzuki, Takekazu Nagae, Shogo Tomida, Masaru Yokota, Kiyoshi Nogi

*Corresponding author for this work

Research output: Contribution to journalArticlepeer-review

Abstract

The present study deals with the fabrication of the zirconium nitride (ZrN) composite with a dispersion of hexagonal boron nitride (h-BN) and with the tribological behavior thereof. Mixture powders were milled for 180 ks or less by a planetary ball mill. The pulse current pressure sintering (PCPS) method was employed in order to consolidate the mixed powders. The sintered compact of ZrN-5 mass% h-BN powders milled for 180 ks shows high density consolidation having a relative density of 92%. Sliding friction tests between sintered compacts of composite ceramics and SUJ-2 steel ball were performed using a ball-on-disc apparatus, in order to estimate the tribological characteristics of sintered compacts by the friction coefficient evolution. Only a 5% addition of h-BN into the ZrN matrix showed a marked decrease in the friction coefficient to about 0.2, preventing adhesive wear. The sintered compact of ZrN-5 mass% h-BN powders milled for 180 ks maintained low friction coefficient for two-times longer compared to the sintered compared of ZrN-5 mass% h-BN mixed powders. However, finger dispersion of h-BN particle under the range of nanometer size is essential to sustain the self-lubricant effect for longer time to be practical.

Original languageEnglish
Pages (from-to)915-921
Number of pages7
JournalFuntai Oyobi Fummatsu Yakin/Journal of the Japan Society of Powder and Powder Metallurgy
Volume49
Issue number10
DOIs
StatePublished - 2002/10

Keywords

  • Ball-on-disc apparatus
  • Hexagonal boron nitride
  • Mechanical milling
  • Pulse current pressure sintering
  • Zirconium nitride

ASJC Scopus subject areas

  • Mechanical Engineering
  • Industrial and Manufacturing Engineering
  • Metals and Alloys
  • Materials Chemistry

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